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RAS Chemistry & Material ScienceЖурнал неорганической химии Russian Journal of Inorganic Chemistry

  • ISSN (Print) 0044-457X
  • ISSN (Online) 3034-560X

Phase equilibria, crystal structure and oxygen nonstoichiometry of complex oxides formed in the system GdCoO3–SrCoO3–δ–SrFeO3–δ–GdFeO3

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PII
10.31857/S0044457X24070142-1
DOI
10.31857/S0044457X24070142
Publication type
Article
Status
Published
Authors
Т. V. Aksenova
  • Affiliation: Yeltsin Ural Federal University
Volume/ Edition
Volume 69 / Issue number 7
Pages
1052-1062
Abstract
The phase equilibria in the quasi-quaternary GdCoO3–SrCoO3–δ–SrFeO3–δ–GdFeO3 system have been studied at 1373 K in air. The homogeneity ranges and crystal structure of solid solutions of general composition Gd1–xSrxCo1–yFeyO3–δ have been determined. Depending on the concentration of introduced strontium and iron, the Gd1–xSrxCo1–yFeyO3–δ oxides crystallize in orthorhombic (x = 0.1 and 0.4 ≤ y ≤ 1.0; x = 0.2 and y = 0.9, sp. gr. Pbnm), tetragonal (0.6 ≤ x ≤ 0.8 and 0.1 ≤ y ≤ 0.5, sp. gr. I4/mmm) or cubic (x = 0.9 and 0.1 ≤ y ≤ 0.9; 0.6 ≤ x ≤ 0.8 and 0.6 ≤ y ≤ 0.9, sp. gr. Pm-3m) perovskite structure. Structural parameters were determined for all single-phase samples. An increase in the concentration of strontium and iron leads to an increase in the unit cell parameters of the Gd1–xSrxCo1–yFeyO3–δ oxides. It has been shown that the oxygen content in Gd1–xSrxCo1–yFeyO3–δ cobaltites, determined by thermogravimetric analysis, decreases with increasing temperature and strontium content in the samples. An isobaric-isothermal phase diagram of the GdCoO3 – SrCoO3–δ–SrFeO3–δ–GdFeO3 system at 1373 K in air was constructed.
Keywords
сложные оксиды рентгенофазовый анализ кристаллическая структура термогравиметрический анализ кислородная нестехиометрия диаграмма состояния
Date of publication
15.07.2024
Year of publication
2024
Number of purchasers
0
Views
25

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