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RAS Chemistry & Material ScienceЖурнал неорганической химии Russian Journal of Inorganic Chemistry

  • ISSN (Print) 0044-457X
  • ISSN (Online) 3034-560X

Synthesis, Ion-Exchange and Photocatalytic Properties of Layered Perovskite-Like CsBa2Nb3O10 Niobate: Comparative Analysis with Related AA′2Nb3O10 Dion-Jacobson Phases (A = K, Rb, Cs; A′ = Ca, Sr, Pb)

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PII
10.31857/S0044457X24030112-1
DOI
10.31857/S0044457X24030112
Publication type
Article
Status
Published
Authors
S. A. Kurnosenko
  • Affiliation: Saint Petersburg State University
Volume/ Edition
Volume 69 / Issue number 3
Pages
373-384
Abstract
Layered perovskite-like niobate CsBa2Nb3O10 has been synthesized in a pure single-phase state for the first time using both nitrates and carbonates of cesium and barium. Unlike its Ca-, Sr- and Pb-containing analogues, the niobate obtained was shown not to undergo substitution of interlayer alkali cations with protons (protonation) upon acid treatments under various conditions. A potential reason for its chemical inactivity may consist in partial disordering of cesium and barium cations between the interlayer space and perovskite slab, hindering the interlayer ion exchange. Optical bandgap energy of CsBa2Nb3O10, being equal to 2.8 eV, potentially allows using visible light (λ < 443 nm) for driving photocatalytic reactions. However, the photocatalytic potential of this niobate towards hydrogen production remains untapped since the activity of the interlayer space in protonation and hydration reactions, as shown earlier, is a fundamentally important factor determining the photocatalytic performance of ion-exchangeable layered perovskite-like oxides.
Keywords
разупорядочение протонирование гидратация фотокатализ водород
Date of publication
17.09.2025
Year of publication
2025
Number of purchasers
0
Views
12

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