Везде

RAS Chemistry & Material ScienceЖурнал неорганической химии Russian Journal of Inorganic Chemistry

  • ISSN (Print) 0044-457X
  • ISSN (Online) 3034-560X

Study of the Structure and Properties of Magnetic Nanopowders of Magnetite-Maggemite Series Solid Solutions by SAPNS

You can
PII
10.31857/S0044457X24030096-1
DOI
10.31857/S0044457X24030096
Publication type
Article
Status
Published
Authors
О. А. Шилова
  • Affiliation:
    Institute of Silicate Chemistry of Russian Academy of Sciences
    Petersburg Nuclear Physics Institute named by B.P. Konstantinov of the Kurchatov Institute
Volume/ Edition
Volume 69 / Issue number 3
Pages
350-363
Abstract
Nanopowders of the magnetite-maggemite series were synthesized by both aqueous precipitation and using sol-gel technology. A comprehensive comparative study of the structure of the synthesized powders was carried out using the methods of X-ray phase analysis (XPA), scanning electron microscopy (SEM), low-temperature nitrogen adsorption and small-angle polarized neutron scattering (SAPNS). It has been established that the synthesized iron oxide nanopowders are porous systems that, depending on the synthesis method, have a one-level or two-level (for powders obtained by aqueous synthesis) and three-level (for powders obtained by the sol-gel method) hierarchical structure organization with different characteristic scales and types of aggregation for each from structural levels, and the characteristic size for the larger level in both cases exceeds 45 nm. It was revealed that the magnetic structure of the obtained iron oxide powders, regardless of the synthesis method, consists of superparamagnetic particles with a characteristic magnetic radius RМ ≈ 4 nm and magnetic-nuclear cross-correlations RMN ≈ 3 nm for powders obtained by the sol-gel method; and with RM ≈ 5–11 nm and RMN ≈ 4–8 nm for powders obtained by aqueous synthesis, depending on the production conditions.
Keywords
оксиды железа  магнитная структура малоугловое рассеяние поляризованных нейтронов метод осаждения золь-гель метод
Date of publication
15.03.2024
Year of publication
2024
Number of purchasers
0
Views
31

References

  1. 1. Ferreira M.I., Cova T., Paixão J.A. et al. // Woodhead Publishing Series in Electronic and Optical Materials. Magnetic Nanoparticle-Based Hybrid Materials. Woodhead Publ, 2021. P. 273. https://doi.org/10.1016/B978-0-12-823688-8.00033-8
  2. 2. Imran M., Shaik A.H., Ansari A.R. et al. // RSC Adv. 2018. V. 8. № 25. P. 13970. https://doi.org/10.1039/C7RA13467C
  3. 3. Rashid H., Mansoor M.A., Haider B. et al. // Sep. Sci. Technol. 2020. V. 55. № 6. P. 1207. https://doi.org/10.1080/01496395.2019.1585876
  4. 4. Aphesteguy J.C., Kurlyandskaya G.V., Celis J.P. et al. // Mater. Chem. Phys. 2015. V. 161. Р. 243. https://doi.org/10.1016/j.matchemphys.2015.05.044
  5. 5. Nazari M., Ghasemi N., Maddah H. et al. // J. Nanostruct. Chem. 2014. V. 4. № 2. P. 99. https://doi.org/10.1007/s40097-014-0099-9
  6. 6. Ramos Guivar J.A., Martínez A.I., Anaya A.O. et al. // Adv. Nanopart. 2014. V. 3. № 3. P. 114. https://doi.org/10.4236/anp.2014.33016
  7. 7. Fedorenko N.Yu., Abiev R.Sh., Kudryashova Yu.S. et al. // Ceram. Int. 2022. V. 48. № 9. P. 13006. https://doi.org/10.1016/j.ceramint.2022.01.174
  8. 8. Шилова О.А., Николаев А.М., Коваленко А.С. и др. // Журн. неорган. химии. 2020. Т. 65. № 3. С. 398.
  9. 9. Коваленко А.С., Шилова О.А., Николаев А.М. и др. // Коллоид. журнал. 2023. Т. 85. № 3. С. 319.
  10. 10. Gopinath S., Philip J. // Mater. Chem. Phys. 2014. V. 145. № 1–2. P. 213. https://doi.org/10.1016/j.matchemphys.2014.02.005
  11. 11. Zienkiewicz-Strzałka M., Skibińska M., Pikus S. // Nucl. Instrum. Methods., Sect. B. 2017. V. 411. P. 72. https://doi.org/10.1016/j.nimb.2017.03.028
  12. 12. Nirschl H., Guo X. // Chem. Eng. Res. Des. 2018. V. 136. P. 431. https://doi.org/10.1016/j.cherd.2018.06.012
  13. 13. Shilova O.A., Nikolaev A.M., Kovalenko A.S. et al. // Ceram. Int. 2021. V. 47. № 20. P. 28866. https://doi.org/10.1016/j.ceramint.2021.07.047
  14. 14. Khamova T.V., Kopitsa G.P., Nikolaev A.M. et al. // Biointer. Res. Appl. Chem. 2021. V. 11. № 4. P. 12285. https://doi.org/10.33263/BRIAC114.1228512300
  15. 15. Danks A.E., Hall S.R., Schnepp Z. // Mater. Horiz. 2016. V. 3. № 2. P. 91. https://doi.org/10.1039/c5mh00260e
  16. 16. Okorokov A.I., Runov V.V. // Physica B. 2001. V. 297. № 1–4. P. 239. https://doi.org/10.1016/S0921-4526 (00)00843-7
  17. 17. Fitzsimmons M.R., Schuller I.K. // J. Magn. Magn. Mater. 2014. V. 350. P. 199. https://doi.org/10.1016/j.jmmm.2013.09.028
  18. 18. Muhlbauer S., Honecker D., P´erigo E.A. et al. // Rev. Mod. Phys. 2019. V. 91. № 1. P. 015004. https://doi.org/10.1103/RevModPhys.91.015004
  19. 19. Honecker D., Bersweiler M., Erokhin S. et al. // Nanoscale Adv. 2022. V. 4. № 4. P. 1026. https://doi.org/10.1039/D1NA00482D
  20. 20. Lee S.H., Lee D.H., Jung H. et al. // Curr. Appl. Phys. 2015. V. 15. № 8. P. 915. https://doi.org/10.1016/j.cap.2015.04.003
  21. 21. Bergenti I., Deriu A., Savini L. et al. // J. Magn. Magn. Mater. 2003. V. 262. № 1. P. 60. https://doi.org/10.1016/S0304-8853 (03)00019-2
  22. 22. Grigoriev S.V., Maleyev S.V., Okorokov A.I. et al. // Europhys. Lett. 2003. V. 63. № 1. Р. 56. https://doi.org/10.1209/epl/i2003-00477-3
  23. 23. Khamova T.V., Shilova O.A., Gorshkova Yu.E. et al. // Nanosystems: Phys. Chem. Math. 2022. V. 13. № 4. P. 414. https://doi.org/10.17586/2220-8054-2022-13-4-414-429
  24. 24. Рунов В.В., Бугров А.Н., Смыслов Р.Ю. и др. // Журн. неорган. химии. 2021. Т. 66. № 2. С. 229.
  25. 25. Fu Z., Xiao Y., Feoktystov A. et al. // Nanoscale. 2016. V. 8. № 43. P. 18541. https://doi.org/10.1039/c6nr06275j
  26. 26. Zákutná D., Nižňanský D., Barnsley L.C. et al. // Phys. Rev. X. 2020. V. 10. № 3. P. 031019. https://doi.org/10.1103/PhysRevX.10.031019
  27. 27. Köhler T., Feoktystov A., Petracic O. et al. // Nanoscale. 2021. V. 13. № 4. P. 6965. https://doi.org/10.1039/d0nr08615k
  28. 28. Chouhan R.S., Horvat M., Ahmed J. et al. // Cancers. 2021. V. 13. № 9. Р. 2213. https://doi.org/10.3390/cancers13092213
  29. 29. Tran H.-V., Ngo N.M., Medhi R. et al. // Materials. 2022. V. 15. № 2. P. 503. https://doi.org/10.3390/ma15020503
  30. 30. Kovalenko A.S., Nikolaev A.M., Khamova T.V. et al. // Glass Phys. Chem. 2021. V. 47. № 1. Р. 67. https://doi.org/10.1134/S1087659621070063
  31. 31. Shilova O.A., Panova G.G., Nikolaev A.M. et al. // Lett. Appl. NanoBioScience. 2021. V. 10. № 2. P. 2215. https://doi.org/10.33263/LIANBS102.22152239
  32. 32. Wang Y., Wang S., Xu M. et al. // Environ. Pollut. 2019. V. 249. P. 1011. https://doi.org/10.1016/j.envpol.2019.03.119
  33. 33. Serpoush M., Kiyasatfar M., Ojaghi J. // Mater. Today: Proc. 2022. V. 65. Part 6. P. 2915. https://doi.org/10.1016/j.matpr.2022.06.441
  34. 34. Turrina Ch., Klassen A., Milani D. et al. // Heliyon. 2023. V. 9. № 6. Р. e16487. https://doi.org/10.1016/j.heliyon.2023.e16487
  35. 35. Baabu P.R.S., Kumar H.K., Gumpu M.B. et al. // Materials. 2023. V. 16. № 1. P. 59. https://doi.org/10.3390/ma16010059
  36. 36. Ibarra J., Melendres J., Almada M. et al. // Mater. Res. Exp. 2015. V. 2. № 9. Р. 095010. https://doi.org/10.1088/2053-1591/2/9/095010
  37. 37. Nasrazadani S., Raman A. // Corros. Sci. 1993. V. 34. № 8. P. 1355. https://doi.org/10.1016/0010-938X (93)90092-U
  38. 38. Pecharroman C., Gonzalez-Carreno T., Iglesias J.E. // Phys. Chem. Miner. 1995. V. 22. P. 21. https://doi.org/10.1007/BF00202677
  39. 39. Anthony J.W., Bideaux R.A., Bladh K.W. Magnetite. Handbook of mineralogy. Chantilly, VA: Mineralogical Society of America, 2018.
  40. 40. Jülich Centre for Neutron Science, QtiKWS 2019. Available online: www.qtisas.com
  41. 41. Жерновой А.И., Дьяченко С.В. // Журн. техн. физики. 2015. Т. 85. № 4. С. 118.
  42. 42. Schaefer D.W., Justice R.S. // Macromolecules. 2007. V. 40. № 24. P. 8501. https://doi.org/10.1021/ma070356w
  43. 43. Баранчиков А.Е., Копица Г.П., Ёров Х.Э. и др. // Журн. неорган. химии. 2021. Т. 66. № 6. С. 774.
  44. 44. Koizumi S., Yue Z., Tomita Y. et al. // Eur. Phys. J. E. 2008. V. 26. № 1–2. P. 137. https://doi.org/10.1140/epje/i2007-10259-3
  45. 45. Guinier A., Fournet G., Walker C.B., Yudowitch K.L. Small-Angle Scattering of X-rays. New York: Wiley, 1955.
  46. 46. Beaucage G., Ulibarri T.A., Black E.P. et al. Hybrid Organic-Inorganic Composites / Eds. By Mark J. et al. ACS Symposium Series; American Chemical Society: Washington, DC, 1995.
  47. 47. Štěpánek M., Matějíček P., Procházka K. et al. // Langmuir. 2011. V. 27. № 9. P. 5275. https://doi.org/10.1021/la200442s
  48. 48. Bale H.D., Schmidt P.W. // Phys. Rev. Lett. 1984. V. 53. № 6. P. 596. https://doi.org/10.1103/PhysRevLett.53.596
  49. 49. Beaucage G. // J. Appl. Crystallogr. 1995. V. 28. № 6. P. 717. https://doi.org/10.1107/S0021889895005292
  50. 50. Ivanova L.A., Ustinovich K.B., Khamova T.V. et al. // Materials. 2020. V. 13. № 9. P. 2087. https://doi.org/10.3390/ma13092087
  51. 51. Larsson P.T., Stevanic-Srndovic J., Roth S.V. et al. // Cellulose. 2022. V. 29. № 1. P. 117. https://doi.org/10.1007/s10570-021-04291-x
  52. 52. Guild J.D., Knox S.T., Burholt S.B. et al. // Macromolecules. 2023. V. 56. № 16. P. 6426. https://doi.org/10.1021/acs.macromol.3c00585
  53. 53. Porod G. // Kolloid-Zeitschrift. 1952. V. 125. № 1. P. 51. https://doi.org/10.1007/BF01519615
  54. 54. Hammouda B. // J. Appl. Crystallogr. 2010. V. 43. № 4. P. 716. https://doi.org/10.1107/S0021889810015773
  55. 55. Schmidt P.W., Avnir D., Levy D. et al. // J. Chem. Phys. 1991. V. 94. № 2. P. 1474. https://doi.org/10.1063/1.460006
QR
Translate

Индексирование

Scopus

Scopus

Scopus

Crossref

Scopus

Higher Attestation Commission

At the Ministry of Education and Science of the Russian Federation

Scopus

Scientific Electronic Library