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RAS Chemistry & Material ScienceЖурнал неорганической химии Russian Journal of Inorganic Chemistry

  • ISSN (Print) 0044-457X
  • ISSN (Online) 3034-560X

Synthesis and Structure of Cyclometallated Palladium Binuclear Complexes with Bridging Carboxylate Ligands

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PII
10.31857/S0044457X2360127X-1
DOI
10.31857/S0044457X2360127X
Publication type
Status
Published
Authors
Yu. E. Makarevich
  • Affiliation: Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences
Volume/ Edition
Volume 68 / Issue number 9
Pages
1244-1254
Abstract
New bimetallic pivalate Pd(II) complex [PdNi(OOCtBu)4(HOOCtBu)] (I) has been synthesized from [PdNi(OOCMe)4] and used as a starting reagent in a further complexation reaction. Cyclometallated binuclear carboxylate palladium complexes [(OOCMe)Pd(2‑phpy)]2 (II) and [(OOCtBu)Pd(2‑phpy)]2 (III) have been obtained by the reaction between heterometallic compounds [Pd(OOCR)4Ni] (R = Me, tBu) and 2-phenylpyridine (2-phpy). The reaction proceeds at room temperature under mild conditions. All the compounds obtained have been isolated in crystalline form from a medium of nonpolar solvents, characterized by single-crystal X-ray diffraction analysis, and deposited at the Cambridge Crystallographic Data Center (CCDC nos. 2256606 for I, 2247942 for II, and 2247943 for III).
Keywords
гетерометаллические комплексы палладий циклометаллирование карбоксилаты биядерные соединения синтез 2-фенилпиридин рентгеноструктурный анализ
Date of publication
01.09.2023
Year of publication
2023
Number of purchasers
0
Views
46

References

  1. 1. Bruce M.I. // Angew. Chem. Int. Ed. Engl. 1977. V. 16. № 2. P. 73.
  2. 2. Albrecht M. // Chem. Rev. 2010. V. 110. № 2. P. 576.
  3. 3. Tamayo A.B., Garon S., Sajoto T. et al. // Inorg. Chem. 2005. V. 44. № 24. P. 8723.
  4. 4. Mayo E.I., Kilså K., Tirrell T. et al. // Photochem. Photobiol. Sci. 2006. V. 5. № 10. P. 871.
  5. 5. Jin C., Liang F., Wang J. et al. // Angew. Chem. Int. Ed. 2020. V. 59. № 37. P. 15987.
  6. 6. Lavrova M.A., Lunev A.M., Goncharenko V.E. et al. // Russ. J. Coord. Chem. 2022. V. 48. № 6. P. 353.
  7. 7. Kopchuk D.S., Slepukhin P.A., Taniya O.S. et al. // Russ. J. Coord. Chem. 2022. V. 48. № 7. P. 430.
  8. 8. Higgins J. // J. Inorg. Biochem. 1993. V. 49. № 2. P. 149.
  9. 9. Qin Q.-P., Zou B.-Q., Tan M.-X. et al. // Inorg. Chem. Commun. 2018. V. 96. P. 106.
  10. 10. Cao J.-J., Zheng Y., Wu X.-W. et al. // J. Med. Chem. 2019. V. 62. № 7. P. 3311.
  11. 11. Yuan H., Han Z., Chen Y. et al. // Angew. Chem. 2021. V. 60. P. 8174.
  12. 12. Dudkina Y.B., Kholin K.V., Gryaznova T.V. et al. // Dalton Trans. 2017. V. 46. № 1. P. 165.
  13. 13. Zakharov A.Yu., Kovalenko I.V., Meshcheriakova E.A. et al. // Russ. J. Coord. Chem. 2022. V. 48. № 12. P. 846.
  14. 14. Powers D.C., Ritter T. // Acc. Chem. Res. 2012. V. 45. № 6. P. 840.
  15. 15. Sprouse S., King K.A., Spellane P.J. et al. // J. Am. Chem. Soc. 1984. V. 106. № 22. P. 6647.
  16. 16. Orwat B., Oh M.J., Zaranek M. et al. // Inorg. Chem. 2020. V. 59. № 13. P. 9163.
  17. 17. Fecková M., Kahlal S., Roisnel T. et al. // Eur. J. Inorg. Chem. 2021. V. 2021. № 16. P. 1592.
  18. 18. Albert J., Janabi B.A., Granell J. et al. // J. Organomet. Chem. 2023. V. 983. P. 122555.
  19. 19. Aiello I., Crispini A., Ghedini M. et al. // Inorg. Chim. Acta. 2000. V. 308. № 1. P. 121.
  20. 20. Davies D.L., Donald S.M.A., Macgregor S.A. // J. Am. Chem. Soc. 2005. V. 127. № 40. P. 13754.
  21. 21. Bercaw J.E., Durrell A.C., Gray H.B. et al. // Inorg. Chem. 2010. V. 49. № 4. P. 1801.
  22. 22. Kozitsyna N.Yu., Nefedov S.E., Dolgushin F.M. et al. // Inorg. Chim. Acta. 2006. V. 359. № 7. P. 2072.
  23. 23. Nefedov S.E., Perova E.V., Yakushev I.A. et al. // Inorg. Chem. Commun. 2009. V. 12. № 6. P. 454.
  24. 24. Nefedov S.E., Kozitsyna N.Yu., Vargaftik M.N. et al. // Polyhedron. 2009. V. 28. № 1. P. 172.
  25. 25. Armarego W.L.F., Chai C.L.L. Purification of laboratory chemicals, 6th ed. Amsterdam, Boston: Elsevier/Butterworth-Heinemann, 2009.
  26. 26. APEX II and SAINT. Madison (Wisconsin, USA): Bruker AXS Inc., 2007.
  27. 27. Krause L., Herbst-Irmer R., Sheldrick G.M. et al. // J. Appl. Cryst. 2015. V. 48. № 1. P. 3.
  28. 28. Sheldrick G.M. // Acta Crystallogr., Sect. A: Found Adv. 2015. V. 71. № 1. P. 3.
  29. 29. Sheldrick G.M. // Acta Crystallogr., Sect. C: Struct. Chem. 2015. V. 71. № 1. P. 3.
  30. 30. Flack H.D. // Acta Crystallogr., Sect. A. 1983. V. 39. № 6. P. 876.
  31. 31. Parsons S., Flack H.D., Wagner T. // Acta Crystallogr., Sect. B. 2013. V. 69. № 3. P. 249.
  32. 32. Dolomanov O.V., Bourhis L.J., Gildea R.J. et al. // J. Appl. Cryst. 2009. V. 42. № 2. P. 339.
  33. 33. Carole W.A., Colacot T.J. // Chem. Eur. J. 2016. V. 22. № 23. P. 7686.
  34. 34. Milani B., Alessio E., Mestroni G. et al. // J. Chem. Soc., Dalton Trans. 1994. № 13. P. 1903.
  35. 35. Kravtsova S.V., Romm I.P., Stash A.I. et al. // Acta Crystallogr., Sect. C. 1996. V. 52. № 9. P. 2201.
  36. 36. Yakushev I.A., Stebletsova I.A., Cherkashina N.V. et al. // J. Struct. Chem. 2021. V. 62. № 9. P. 1411.
  37. 37. Ukhin L.Yu., Dolgopolova N.A., Kuz’mina L.G. et al. // J. Organomet. Chem. 1981. V. 210. № 2. P. 263.
  38. 38. Yakushev I.A., Ogarkova N.K., Sosunov E.A. et al. // J. Struct. Chem. 2023. V. 64. № 3. P. 377.
  39. 39. Stolarov I.P., Yakushev I.A., Churakov A.V. et al. // Inorg. Chem. 2018. V. 57. № 18. P. 11482.
  40. 40. Markov P.V., Bragina G.O., Baeva G.N. et al. // Kinet Catal. 2016. V. 57. № 5. P. 617.
  41. 41. Kozitsyna N.Yu., Nefedov S.E., Dolgushin F.M. et al. // Inorg. Chim. Acta. 2006. V. 359. № 7. P. 2072.
  42. 42. Akhmadullina N.S., Cherkashina N.V., Kozitsyna N.Yu. et al. // Inorg. Chim. Acta. 2009. V. 362. № 6. P. 1943.
  43. 43. Markov A.A., Klyagina A.P., Dolin S.P. et al. // Russ. J. Inorg. Chem. 2009. V. 54. № 6. P. 885.
  44. 44. Lord R.C., Merrifield R.E. // J. Chem. Phys. 1953. V. 21. № 1. P. 166.
  45. 45. Kozitsyna N.Yu., Nefedov S.E., Yakushev I.A. et al. // Mendeleev Commun. 2007. V. 17. № 5. P. 261.
  46. 46. Thu H.-Y., Yu W.-Y., Che C.-M. // J. Am. Chem. Soc. 2006. V. 128. № 28. P. 9048.
  47. 47. Dinçer M., Özdemir N., Günay M.E. et al. // Acta Crystallogr., Sect. E: Struct. Rep. Online. 2008. V. 64. № 2. P. M381.
  48. 48. Kim M., Taylor T.J., Gabbaï F.P. // J. Am. Chem. Soc. 2008. V. 130. № 20. P. 6332.
  49. 49. Atla S.B., Kelkar A.A., Puranik V.G. et al. // J. Organomet. Chem. 2009. V. 694. № 5. P. 683.
  50. 50. Fairlamb I.J.S. // Angew. Chem. Int. Ed. 2015. V. 54. № 36. P. 10415.
  51. 51. Cherkashina N.V., Churakov A.V., Yakushev I.A. et al. // Russ. J. Coord. Chem. 2019. V. 45. № 4. P. 253.
  52. 52. Yakushev I.Ya., Gekhman A.E., Klyagina A.P. et al. // Russ. J. Coord. Chem. 2016. V. 42. № 9. P. 604.
  53. 53. Shishilov O.N., Kumanyaev I.M., Akhmadullina N.S. et al. // Inorg. Chem. Commun. 2015. V. 58. P. 16.
  54. 54. Elumalai P., Thirupathi N., Nethaji M. // J. Organomet. Chem. 2013. V. 741–742. P. 141.
  55. 55. Wakioka M., Nakamura Y., Wang Q. et al. // Organomet. 2012. V. 31. № 13. P. 4810.
  56. 56. Cordero B., Gómez V., Platero-Prats A.E. et al. // Dalton Trans. 2008. № 21. P. 2832.
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