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RAS Chemistry & Material ScienceЖурнал неорганической химии Russian Journal of Inorganic Chemistry

  • ISSN (Print) 0044-457X
  • ISSN (Online) 3034-560X

Supramolecular Hybrid Complexes Based on Octahedral Molybdenum(II) Iodide Cluster and Zinc(II) Porphyrin

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PII
10.31857/S0044457X23600743-1
DOI
10.31857/S0044457X23600743
Publication type
Status
Published
Authors
M. V. Volostnykh
  • Affiliation:
    Frumkin Institute of Physical Chemistry and Electrochemistry, Russian Academy of Sciences
    Department of Fundamental Physical and Chemical Engineering, Moscow State University
    Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Scie
Volume/ Edition
Volume 68 / Issue number 9
Pages
1192-1201
Abstract
The possibility of the formation of supramolecular hybrids based on two photosensitizers, an octahedral molybdenum(II) iodide cluster with six terminal isonicotinate ligands (Bu4N)2[{Mo6I8}(OOC–C5H4N)6] (PyMoC, C) and A4-type zinc(II) porphyrin (ZnTPP, P), has been demonstrated. Spectrophotometric and NMR titration methods have shown that the formation of CPn complexes (n = 1–6) occurs in solutions of noncoordinating chlorinated solvents due to the formation of metal–N-ligand coordination bonds between the components. The use of an octahedral cluster as a hexatopic N-ligand and the lability of the Zn···NPy bonds together lead to the formation of a series of CPn complexes (n = 1–6), which are in dynamic equilibrium in solution. Nevertheless, conditions have been selected to isolate single crystals of individual forms CP4 + 2 and CP6 + 2, and their structures have been determined by X-ray diffraction analysis. The PyMoC cluster turns out to coordinate four or six ZnTPP molecules, respectively, while both structures contain two “extramolecules” of zinc(II) porphyrin bound to the cluster via hydrogen bonds involving the oxygen atoms of the isonicotinate groups and protons of water axially coordinated to the porphyrin metal center.
Keywords
порфирин гексаядерный галогенидный кластер молибдена(II) координационная химия органо-неорганические материалы рентгеноструктурный анализ
Date of publication
01.09.2023
Year of publication
2023
Number of purchasers
0
Views
42

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