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RAS Chemistry & Material ScienceЖурнал неорганической химии Russian Journal of Inorganic Chemistry

  • ISSN (Print) 0044-457X
  • ISSN (Online) 3034-560X

Transformations of Cerium Tetrafluoride Hydrate under Hydrothermal Conditions: A New Cerium Fluoride Hydrate Се3F10 ⋅ 3Н2О

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PII
10.31857/S0044457X23600688-1
DOI
10.31857/S0044457X23600688
Publication type
Status
Published
Authors
A. E. Baranchikov
  • Affiliation: Kurnakov Institute of General and Inorganic Chemistry, Russian Academy of Sciences
Volume/ Edition
Volume 68 / Issue number 10
Pages
1348-1357
Abstract
The behavior of cerium tetrafluoride hydrate was studied in water at a temperature of 80°C and under hydrothermal treatment at 100, 130, and 220°C for a day. The product of the hydrothermal treatment of CeF4·H2O at 100°C was investigated by chemical, thermogravimetric, IR spectroscopic, and X-ray powder diffraction analyses, which identified a new cerium fluoride with the composition, presumably, Ce3F10⋅3H2O or, most likely, (H3O)Ce3F10⋅2H2O. New compound crystallizes in the space group with a unit cell parameter of 11.66 Å. Hydrothermal treatment of cerium tetrafluoride hydrate at temperatures above 130°C leads to hydrolysis and reduction of cerium(IV) fluoride compounds to form CeO2 and CeF3.
Keywords
тетрафторид церия трифторид церия диоксид церия редкоземельные элементы
Date of publication
01.10.2023
Year of publication
2023
Number of purchasers
0
Views
51

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