- PII
- 10.31857/S0044457X23600275-1
- DOI
- 10.31857/S0044457X23600275
- Publication type
- Status
- Published
- Authors
- Volume/ Edition
- Volume 68 / Issue number 7
- Pages
- 975-987
- Abstract
- Cs2O–Al2O3 ceramic samples containing 20 and 33 mol % cesium oxide were prepared by сeramic technique and by the glycine–nitrate combustion process. The prepared samples were identified and characterized by X-ray powder diffraction and X-ray fluorescence analyses, scanning electron microscopy, and differential thermal analysis. X-ray powder diffraction and scanning electron microscopy showed that the phase composition and surface of the samples change significantly and nonmonotonically depending on the synthetic method used and the heat treatment parameters of the batch. Optimal synthetic conditions and heat treatment parameters for preparing Cs2O–Al2O3 samples were elucidated.
- Keywords
- Date of publication
- 17.09.2025
- Year of publication
- 2025
- Number of purchasers
- 0
- Views
- 11
References
- 1. Prins R. // J. Catal. 2020. V. 392. P. 336. https://doi.org/10.1016/j.jcat.2020.10.010
- 2. Busca G. // Prog. Mater. Sci. 2019. V. 104. P. 215. https://doi.org/10.1016/j.pmatsci.2019.04.003
- 3. Meephoka C., Chaisuk C., Samparnpiboon P., Praserthdam P. // Catal. Commun. 2008. V. 9. P. 546. https://doi.org/10.3390/cryst11060690
- 4. Shreyas P.S., Mahesh B.P., Rajanna S., Rajesh N. // Mat. Tood. Proc. 2021. V. 45. P. 429. https://doi.org/10.1016/j.matpr.2020.12.1012
- 5. Подзорова Л.И., Ильичёва А.А., Пенькова О.И. и др. // Неорган. материалы. 2019. Т. 55. С. 671. https://doi.org/0.1134/S0002337X19060125
- 6. Chaitree W., Jiemsirilers S., Mekasuwandumrong O. et al. // Catal. Today. 2011. V. 164. P. 302. https://doi.org/10.1016/j.cattod.2010.11.004
- 7. Tsybulya S.V., Kryukova G.N. // Phys. Rev. B. 2008. V. 77. P. 024112. https://doi.org/10.1103/PhysRevB.77.024112
- 8. Paglia G., Buckley C.E., Rohl A.L. et al. // Phys. Rev. B. 2003. V. 68. P. 144110. https://doi.org/10.1103/PhysRevB.68.144110
- 9. Rudolph M., Motylenko M., Rafaja D. // IUCrJ. 2019. V. 6. P. 116. https://doi.org/10.1107/S2052252518015786
- 10. Marí B., Singh K.C., Moya M. et al. // Opt. Quant. Electr. 2015. V. 47. P. 1569. https://doi.org/10.1007/s11082-014-9997-9
- 11. Saeed Adel M.N., Al-Gunaid Murad Q.A., Subramani N.K. et al. // Pol.-Plast. Tech. Eng. 2018. V. 57. P. 1188. https://doi.org/10.1080/03602559.2017.1373402
- 12. McMillan P.F., Grzechnik A., Chotalla H. // J. Non-Cryst. Solids. 1998. V. 226. № 3. P. 239. https://doi.org/10.1016/S0022-3093 (98)00416-5
- 13. Fukumi K., Sakka S., Kokubo T. // J. Non-Cryst. Solids. 1987. V. 93. P. 190. https://doi.org/10.1016/S0022-3093 (87)80038-8
- 14. Macleod N., Keel J.M., Lambert R.M. // Catal. Lett. 2003. V. 86. P. 51. https://doi.org/10.1023/A:1022602807322
- 15. Ansari A.A., Khan M.A.M., Khan M.N., Alrokayan S.A. // J. Semicond. 2011. V. 32. P. 1. https://doi.org/10.1088/1674-4926/32/4/043001
- 16. Guéneau C., Flèche J.L. // Calphad. 2015. V. 49. P. 67. https://doi.org/10.1016/j.calphad.2015.02.002
- 17. Stolyarova V.L., Vorozhtcov V.A., Lopatin S.I. et al. // Rapid Commun. Mass Spectrom. 2021. V. 35. P. e9079. https://doi.org/10.1002/rcm.9079
- 18. Stolyarova V.L., Vorozhtcov V.A., Lopatin S.I. et al. // Rapid Commun. Mass Spectrom. 2021. V. 35. P. e9097. https://doi.org/10.1002/rcm.9097
- 19. Каймиева О.С., Сабирова И.Э., Буянова Е.С., Петрова С.А. // Журн. неорган. химии. 2022. Т. 67. № 9. С. 1211. https://doi.org/10.31857/S0044457X22090057
- 20. Медведева А.Е., Махонина Е.В., Печень Л.С. и др. // Журн. неорган. химии. 2022. Т. 67. № 7. С. 896. https://doi.org/10.31857/S0044457X22070157
- 21. Babaev E.V. // Russ. J. Gen. Chem. 2010. V. 80. P. 2590. https://doi.org/10.1134/S1070363210120261
- 22. O’Donnell M.J., Zhou C., Scott W.L. // J. Am. Chem. Soc. 1996. V. 118. P. 6070. https://doi.org/10.1021/ja9601245
- 23. Симоненко Т.Л., Симоненко Н.П., Симоненко Е.П., Кузнецов Н.Т. // Журн. неорган. химии. 2022. Т. 67. № 10. С. 1359. https://doi.org/10.31857/S0044457X22600736
- 24. Томилин О.Б., Мурюмин Е.Е., Фадин М.В., Щипакин С.Ю. // Журн. неорган. химии. 2022. Т. 67. № 4. С. 457. https://doi.org/10.31857/S0044457X22040195
- 25. Wang J., Zhao H., Wen Y. // Electrochim. Acta. 2013. V. 113. P. 679. https://doi.org/10.1016/j.electacta.2013.09.086
- 26. Журавлев В.Д., Васильев В Г., Владимирова Е.В. и др. // Физ. хим. стекла. 2010. Т. 36. № 4. С. 632. https://doi.org/10.1134/S1087659610040164
- 27. Cardarelli F. Materials handbook. London: Springer-Verlag, 2008. P. 600.
- 28. Zhou R.-S., Snyder R. // Acta Crystallogr., Sect. B: Struct. Sci. 1991. V. 47. P. 617. https://doi.org/10.1107/S0108768191002719
- 29. Langlet G. // C. R. Acad. Sci. 1964. V. 259. P. 3769.