RAS Chemistry & Material ScienceЖурнал неорганической химии Russian Journal of Inorganic Chemistry

  • ISSN (Print) 0044-457X
  • ISSN (Online) 3034-560X

Hydrothermal Synthesis of Silver Sulfide

PII
10.31857/S0044457X22602000-1
DOI
10.31857/S0044457X22602000
Publication type
Status
Published
Authors
Volume/ Edition
Volume 68 / Issue number 5
Pages
589-596
Abstract
Silver sulfide powders with submicro- and micrometer particle sizes have been synthesized by the hydrothermal method at temperatures from 373 to 453 K in aqueous and alcoholic solutions of silver nitrate, sodium sulfide and citrate, sulfur, and thiocarbamide. The crystal structures of the synthesized powders, morphology, composition, and particle size of silver sulfide have been analyzed by X-ray diffraction, scanning electron microscopy, energy-dispersive X-ray analysis, and gas adsorption. The powder particles have a similar morphology in the form of rectangular parallelepipeds and cubes with smoothed edges; the size of the powder particles depends on the synthesis conditions and ranges from ~500 to 2000 nm.
Keywords
сульфид серебра гидротермальный синтез размер и морфология частиц EDX-анализ
Date of publication
01.05.2023
Year of publication
2023
Number of purchasers
0
Views
46

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