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RAS Chemistry & Material ScienceЖурнал неорганической химии Russian Journal of Inorganic Chemistry

  • ISSN (Print) 0044-457X
  • ISSN (Online) 3034-560X

SYNTHESIS OF NANO-SIZED SnO BY DIRECT CHEMICAL PRECIPITATION USING TIN(II) CHLORIDE

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PII
S3034560XS0044457X25040032-1
DOI
10.7868/S3034560X25040032
Publication type
Article
Status
Published
Authors
N.A. Fisenko
  • Affiliation: Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences
Volume/ Edition
Volume 70 / Issue number 4
Pages
502-510
Abstract
The process of synthesizing nano-sized SnO by direct chemical precipitation using tin(II) chloride and hydrogen peroxide has been investigated. The thermal behavior of the obtained powders was studied using simultaneous thermal analysis (TGA/DSC). The impact of HO concentration in the reaction system on the set of functional groups in the materials was demonstrated using infrared spectroscopy, while X-ray diffraction analysis (XRD) was utilized to examine the crystalline structure of the powders, including the thermal transformation of tin(II) oxyhydroxide. Scanning electron microscopy (SEM) and transmission electron microscopy (TEM) were employed to show the effect of the reaction system composition on the size of primary particles and the agglomerates formed. In particular, it was established that with an increase of HO concentration, both the size of the primary particles and the agglomerates decrease. The roughness of the films formed from the obtained nanopowders was studied using atomic force microscopy (AFM). Kelvin probe force microscopy (KPFM) was used to construct surface potential distribution maps for the obtained materials and to evaluate the electron work function from their surface.
Keywords
диоксид олова оксид олова(IV) оксогидроксид олова хлорид олова(II) химическое осаждение нанопорошок пероксид водорода
Date of publication
15.04.2025
Year of publication
2025
Number of purchasers
0
Views
24

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