- PII
- 10.31857/S0044457X24120116-1
- DOI
- 10.31857/S0044457X24120116
- Publication type
- Article
- Status
- Published
- Authors
- Volume/ Edition
- Volume 69 / Issue number 12
- Pages
- 1785-1795
- Abstract
- For the first time composites based on manganese monoxide of cubic crystal system MnO/C were synthesized by hydrothermal-microwave treatment of aqueous solution of potassium permanganate with ascorbic acid and subsequent annealing of the precursor in an inert atmosphere at temperature of 500℃. It was found that the key parameter determining the features of composite formation is the molar ratio of the reaction mass components equal to Mn : C6H8O6 = 1 : (0.75-1.5). A mechanism of MnO/C composite formation is proposed. The maximum carbon content in the composite material is ≈ 3 wt. %. The main physicochemical characteristics of the synthesized composites were determined using the methods of X-ray phase and thermogravimetric analysis, Raman spectroscopy, scanning electron microscopy, low-temperature nitrogen adsorption. The study of the behavior of MnO/C as an anode material for a lithium-ion battery showed the efficiency of its use only at high current densities.
- Keywords
- углерод композит аскорбиновая кислота гидротермальный синтез анодный материал
- Date of publication
- 15.12.2024
- Year of publication
- 2024
- Number of purchasers
- 0
- Views
- 45
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