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RAS Chemistry & Material ScienceЖурнал неорганической химии Russian Journal of Inorganic Chemistry

  • ISSN (Print) 0044-457X
  • ISSN (Online) 3034-560X

HYDROTHERMAL SYNTHESIS OF HIERARCHICALLY ORGANIZED MoS2 AND THE FORMATION OF FILMS BASED ON IT

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PII
10.31857/S0044457X24120035-1
DOI
10.31857/S0044457X24120035
Publication type
Article
Status
Published
Authors
T. L Simonenko
  • Affiliation: Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences
N. P Simonenko
  • Affiliation: Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences
M. V. Kozlova
  • Affiliation: Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences
Volume/ Edition
Volume 69 / Issue number 12
Pages
1690-1704
Abstract
The influence of hydrothermal synthesis parameters on the crystal structure and morphology of MoS2 particles has been shown. The results of synchronous thermal analysis showed that at the concentration of molybdenum cations of 0.05 mol/L, the increase in the duration of hydrothermal treatment leads to a decrease in the total mass loss (Δm), and the increase in c(Mo), on the contrary, results in a significant increase in the total Δm value. The dependence of the exo-effect maximum position, related to the MoS2 oxidation with the formation of MoO3, on the synthesis conditions was determined. According to X-ray diffraction analysis (XRD) data, the 1T-MoS2 phase is formed at minimum c(Mo) and duration of heat treatment. Increasing the time duration leads to the transformation of 1T-phase into 2H-MoS2. With increasing c(Mo), the 2H-phase transforms to 1T-MoS2 and further to 1T/2H-MoS2. The transformation of MoS2 structure was also analyzed by Raman spectroscopy. From the results of scanning electron microscopy (SEM), all samples represent flower-like nanostructures consisting of twisted nanosheets. According to transmission electron microscopy data, individual nanosheets with a length of 50-500 nm are formed after delamination of molybdenum disulfide structures. The microstructure of the obtained MoS2 film was studied by SEM and atomic force microscopy. Analysis of the film surface by Kelvin-probe force microscopy allows to establish the material has high electrical conductivity, and the work function value of the film surface was calculated.
Keywords
гидротермальный синтез дисульфид молибдена нанолисты иерархические структуры пленки метод вращения подложки электрод суперконденсатор
Date of publication
15.12.2024
Year of publication
2024
Number of purchasers
0
Views
55

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