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RAS Chemistry & Material ScienceЖурнал неорганической химии Russian Journal of Inorganic Chemistry

  • ISSN (Print) 0044-457X
  • ISSN (Online) 3034-560X

SYNTHESIS AND STUDY OF SUBMICRON BARIUM HEXAFERRITE CERAMICS OBTAINED BY LIQUID-PHASELOW-TEMPERATURE SINTERING OF BaFe12O19 NANOPARTICLES

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PII
10.31857/S0044457X24110042-1
DOI
10.31857/S0044457X24110042
Publication type
Article
Status
Published
Authors
A. Yu. Mironovich
  • Affiliation: National University of Science & Technology “MISIS”
M. V. Kozlova
  • Affiliation: Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences
Volume/ Edition
Volume 69 / Issue number 11
Pages
1535-1546
Abstract
In this work, the problem of obtaining ceramic samples of barium hexaferrite BaFe12O19 with high values of coercivity was being solved. For this purpose, BaFe12O19 nanopowder with coercivity Hc=445 kA/m was synthesized by hydrothermal synthesis. Sintering was carried out at low temperature (900∘C) to preserve the grains in a single-domain state. To perform sintering at such a low temperature, B2O3 or Bi2O3 was added to the hexaferrite. The effect of the amount and type of additive on the phase composition, microstructure and magnetic properties of sintered hexaferrite was studied. It was shown that using Bi2O3(in the form of 0.5, 1 or 3 wt.% of Bi(NO3)3) led to no changes in the phase composition, while addition of B2O3(in the form of 0.5, 1 or 3 wt.% of H3BO3) resulted in partial transformation of hexaferrite into hematite α-Fe2O3. It was found that with increasing concentration of Bi2O3 or B2O3, the average grain size of BaFe12O19 increases,but does not exceed the critical single-domain size. This provides high Hcvalues of the sintered samples (370-420 kA/m), which makes them superior to most well-known brands of unsubstituted hexaferrites.
Keywords
гексаферрит бария оксид бора оксид висмута жидкофазное спекание магнитные свойства
Date of publication
15.11.2024
Year of publication
2024
Number of purchasers
0
Views
55

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