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RAS Chemistry & Material ScienceЖурнал неорганической химии Russian Journal of Inorganic Chemistry

  • ISSN (Print) 0044-457X
  • ISSN (Online) 3034-560X

Surface Transformation Of Ultrahigh-Temperature Ceramics HfB2-SiC-C(graphene) Under The Influence Of High-Speed Disossociated Nitrogen Jets

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PII
10.31857/S0044457X24040156-1
DOI
10.31857/S0044457X24040156
Publication type
Article
Status
Published
Authors
E. P. Simonenko
  • Affiliation: Kurnakov Institute of General and Inorganic Chemistry of the Russian Academy of Sciences
Volume/ Edition
Volume 69 / Issue number 4
Pages
594-606
Abstract
In order to study the promising potential of HfB2–30 vol % SiC ultrahigh-temperature ceramic materials modified with low amounts of reduced graphene oxide for the creation of aerospace equipment intended for use in N2-based atmospheres, the effect of high-speed dissociated nitrogen flow on it has been investigated. It has been established that under the chosen conditions of exposure during the stepwise increase of the anode power supply of plasma torch and, accordingly, the influencing heat flux, at certain parameters there is a sharp increase in the surface temperature from ~1750 to 2000-2100°C. At the same time, further increase of the heat flux has no obvious and proportional effect on the temperature of the sample surface, which may indicate its high catalyticity with respect to the reactions of surface recombination of atomic nitrogen. It is shown that the surface layers of the material undergo chemical transformation (removal of silicon-containing substances, formation of a new phase based on HfN), which is accompanied by a significant change in the microstructure (formation of dendrite-like structures), which affects the optical and catalytic characteristics of the surface.
Keywords
UHTC графен HfB2 SiC высокоэнтальпийный поток азота индукционный плазмотрон
Date of publication
17.09.2025
Year of publication
2025
Number of purchasers
0
Views
11

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